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Structural and spectroscopic characterization of CIC(O)SNSO. A theoretical and experimental study
Citation key ISI:000080565200024
Author Romano, R M and Della Vedova, C O and Boese, R and Hildebrandt, P
Pages 2551-2557
Year 1999
ISSN 1463-9076
Address THOMAS GRAHAM HOUSE, SCIENCE PARK, MILTON RD,, CAMBRIDGE CB4 0WF, CAMBS, ENGLAND
Journal Phys. chem. chem. phys
Volume 1
Number 10
Month MAY 15
Publisher ROYAL SOC CHEMISTRY
Abstract {N-(Sulfinylimine)chlorocarbonylsulfane, CIC(O)SNSO, was prepared by the reaction of CIC(O)SCI with Hg(NSO)(2). The crystal structure of CIC(O)SNSO was determined by X-ray diffraction analysis from crystals obtained at low temperature using a miniature zone melting procedure. The molecule exhibits only one form with C-s symmetry: the C=O double bond syn with respect to the S-N single bond, the C-S single bond anti to the N=S double bond and the S-N single bond syn with respect to the S=O double bond. The following skeletal parameters were determined (distances in Angstrom, angles in degrees, errors between parentheses expressed as sigma): Cl-C = 1.771(2)
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