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| Citation key | ISI:000080565200024 |
|---|---|
| Author | Romano, R M and Della Vedova, C O and Boese, R and Hildebrandt, P |
| Pages | 2551-2557 |
| Year | 1999 |
| ISSN | 1463-9076 |
| Address | THOMAS GRAHAM HOUSE, SCIENCE PARK, MILTON RD,, CAMBRIDGE CB4 0WF, CAMBS, ENGLAND |
| Journal | Phys. chem. chem. phys |
| Volume | 1 |
| Number | 10 |
| Month | MAY 15 |
| Publisher | ROYAL SOC CHEMISTRY |
| Abstract | {N-(Sulfinylimine)chlorocarbonylsulfane, CIC(O)SNSO, was prepared by the reaction of CIC(O)SCI with Hg(NSO)(2). The crystal structure of CIC(O)SNSO was determined by X-ray diffraction analysis from crystals obtained at low temperature using a miniature zone melting procedure. The molecule exhibits only one form with C-s symmetry: the C=O double bond syn with respect to the S-N single bond, the C-S single bond anti to the N=S double bond and the S-N single bond syn with respect to the S=O double bond. The following skeletal parameters were determined (distances in Angstrom, angles in degrees, errors between parentheses expressed as sigma): Cl-C = 1.771(2) |
| Bibtex Type of Publication | Article |
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